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agency
meets requirements for USP G36
Quality Level
packaging
bottle of 50 g
parameter
50-300 °C temp. range
technique(s)
gas chromatography (GC): suitable
matrix active group
SE-54 phase
solubility
chloroform: soluble
column type
packed GC
General description
GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients.[1] The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase.[2] SE-54 is good for nonpolar phase as it provides better peak shapes for polar chemicals.[3]
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.
Application
SE-54 is suitable for analysis of polycyclic aromatic hydrocarbons (PAH) and polychlorinated biphenyls (PCB) using PTE-5 fused silica capillary coulmn.[4]
Storage Class
10 - Combustible liquids
wgk_germany
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves
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G Adami et al.
Journal of environmental monitoring : JEM, 2(3), 261-265 (2001-03-21)
A sediment sampling based on a two-dimensional mapping was performed in the harbour of Trieste (northern Adriatic Sea), considering 28 sites exposed to pollutant inputs from harbour and industrial activities. Polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs) were determined
Markku Mesilaakso
Chemical Weapons Convention Chemicals Analysis: Sample Collection, Preparation and Analytical Methods, 187-187 (2005)
Abhijit Ghosh et al.
Journal of chromatography. A, 1517, 134-141 (2017-09-01)
Miniaturization of gas chromatography (GC) instrumentation is of interest because it addresses current and future issues relating to compactness, portability and field application. While incremental advancements continue to be reported in GC with columns fabricated in microchips (referred to in
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
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