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21086

Supelco

GC Stationary Phase

phase β,β-Oxydipropionitrile, bottle of 50 g

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About This Item

EC Number:
UNSPSC Code:
23151817

packaging

bottle of 50 g

parameter

0-75 °C temp. range

technique(s)

gas chromatography (GC): suitable

matrix active group

β,β-Oxydipropionitrile phase

solubility

methanol: soluble

General description

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients.[1] The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase.[2] β,β-Oxydipropionitrile (ODPN) is an organic liquid phase suitable for partition chromatography.[3]
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.

Application

ODPN may be used as stationary liquid phase in an experiemental procedure done in order to cpmpare mixed packing gas chromatography (MPGC) and mixed liquid gas chromatography (MLGC) on the basis of the factore like their retention ability, column efficiency and tailing reducing effect.[4]

Storage Class

10 - Combustible liquids

wgk_germany

WGK 2

flash_point_f

235.4 °F - closed cup

flash_point_c

113 °C - closed cup

ppe

Eyeshields, Gloves


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B. Sivasankar
Biosperations: Principles and Techniques, 166-166 (2005)
Comparison of mixed packing gas chromatography with mixed stationary liquid gas chromatography:Studies of gas chromatography with mixed stationary phase.
MITOOKA Mitsuyuki
Bunseki Kagaku, 21, 867-877 (1972)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)

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