Z731323
Columns for Gas Chromatography: Performance and Selection
for separating and analyzing a wide variety of organic compounds and gases
About This Item
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publication info
E. Barry and R. Grob, John Wiley and sons, 2007, 298 pp., hard cover
manufacturer/tradename
Wiley
General description
This resource includes - Methods of choosing both capillary and packed columns; Selection of dimensions (column length, I.D., film thickness, etc.) and type of column; Guidelines for proper connections of the column to the injector and detector; United States Pharmacopeia and National Formulary chromatographic methods; ASTM, EPA, NIOSH, and OSHA column selection specifications; Information on the advantages of computer assistance in GC and multidimensional GC; Comprehensive information on column oven temperature control.
Table of Contents
2 Packed Column Gas Chromatography
2.1 Introduction
2.2 Solid Supports and Adsorbents
2.3 Stationary Phases
2.4 Column Preparation
2.5 United States Pharmacopeia and National Formulary Chromatographic Methods
References
3 Capillary Column Gas Chromatography
3.1 Introduction
3.2 Capillary Column Technology
3.3 Preparation of Fused-Silica Capillary Columns
3.4 Chromatographic Performance of Capillary Columns
3.5 Stationary-Phase Selection for Capillary Gas Chromatography
3.6 Specialty Columns
3.7 Capillary Column Selection
3.8 Column Installation and Care
3.9 Special Gas Chromatographic Techniques
References
4 Column Oven Temperature Control
4.1 Thermal Performance Variables and Electronic Considerations
4.2 Advantages of Temperature Programming over Isothermal Operation
4.3 Oven Temperature Profiles for Programmed-Temperature Gas Chromatography
4.4 Role of Computer Assistance in Optimizing Separations in Gas Chromatography
4.5 Fast or High-Speed Gas Chromatography
4.6 Subambient Oven Temperature Control
References
Selected References
Appendix A: Guide to Selection of Packed Columns
Appendix B: Column Selection
Index
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