Journal of the American Society for Mass Spectrometry, 24(4), 493-501 (2013-03-21)
The benzoxyl radical is a key intermediate in the combustion of toluene and other aromatic hydrocarbons, yet relatively little experimental work has been performed on this species. Here, a combination of electrospray ionization (ESI), multistage mass spectrometry experiments, and density
Journal of mass spectrometry : JMS, 47(10), 1341-1346 (2012-09-29)
A high-performance liquid chromatography coupled with Q-time of flight mass spectrometry (HPLC/Q-TOF MS) method was developed and validated for the determination of 1, 3-diaminopropane, putrescine, cadaverine, spermidine and spermine in human plasma. The plasma samples were first pretreated by 10%
Chemical communications (Cambridge, England), (8)(8), 1037-1039 (2005-02-19)
Conditions are reported for the facile, high-yielding coupling of acyl chlorides with terminal alkynes in a reaction involving palladium and copper iodide; the reaction is tolerant of a wide variety of acyl chlorides and terminal alkynes and provides a convenient
Journal of hazardous materials, 115(1-3), 91-100 (2004-11-03)
The risks associated with batch processing in the manufacture of chemicals and pharmaceuticals via highly exothermic reactions are of special interest due to the possibility of runaway reactions. o-Nitrated benzoyl chlorides are intermediates in the production of agrochemicals and are
Physical chemistry chemical physics : PCCP, 11(38), 8467-8476 (2009-09-24)
In this contribution we attempt to correlate the dynamical states of water molecules in reverse micelles with a solvolysis reaction in accordance with the activation energy barrier crossing model at the micellar interface. Precise measurement of the different dynamical states
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