1.03296

Chloroform-D1

0.03 vol.% TMS, deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv^™

• Synonym(s): Chloroform-D1, Deuterochloroform
• Empirical Formula (Hill Notation): CCl₃D
• CAS Number: 865-49-6
• Molecular Weight: 120.38
• MDL number: MFCD00000827
• UNSPSC Code: 12142201
• EC Index Number: 212-742-4
• NACRES: NA.22

Properties

• vapor pressure: 211 hPa ( 20 °C)
• Quality Level: 200
• form: liquid
• potency: 695 mg/kg LD₅₀, oral (Rat); >3980 mg/kg LD₅₀, skin (Rabbit)
• technique(s): NMR: suitable
• impurities: ≤0.01% Water (H<SUB>2</SUB>O) (NMR); 0.03% Tetramethylsilane (NMR)
• bp: 60 °C/1013 hPa
• mp: -64.1 °C
• solubility: 4.6 g/L
• density: 1.50 g/cm³ at 20 °C
• storage temp.: 2-8°C
• InChI: 1S/CHCl3/c2-1(3)4/h1H/i1D
• InChI key: HEDRZPFGACZZDS-MICDWDOJSA-N

Description

General description

A wide range of MagniSolv deuterated solvents with extremely low residual water, excellent chemical purity, and the highest isotopic enrichment available can satisfy the most demanding requirements of researchers. Depending on application and sensitivity of the NMR spectrometer our offer solvents with deuteration degrees between 98% and 99.96%. In case of all the water soluble deuterated standard products, water content is specified according to both Karl Fischer and NMR.

Analysis Note

Deuteration degree: ≥ 99.8 %
Water (NMR, H₂O): ≤ 0.01 %
Tetramethylsilane (NMR-spectrum): 0.03%
Performance test (NMR-spectrum): passes test

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Legal Information

MAGNISOLV is a trademark of Merck KGaA, Darmstadt, Germany

Safety Information

• pictograms: GHS06,GHS08
• signalword: Danger
• hcodes: H302 - H315 - H319 - H331 - H336 - H351 - H361d - H372
• pcodes: P202 - P301 + P312 - P302 + P352 - P304 + P340 + P311 - P305 + P351 + P338 - P308 + P313
• Hazard Classifications: Acute Tox. 3 Inhalation - Acute Tox. 4 Oral - Carc. 2 - Eye Irrit. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 1 Oral - STOT SE 3
• target_organs: Central nervous system
• Storage Class: 6.1C - Combustible, acute toxic Cat.3 / toxic compounds or compounds which causing chronic effects
• wgk_germany: WGK 3