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  • Veterinary drug residues in domestic and imported foods of animal origin in the Republic of Korea.

Veterinary drug residues in domestic and imported foods of animal origin in the Republic of Korea.

Food additives & contaminants. Part B, Surveillance (2014-12-30)
JeongWoo Kang, Hae-Chul Park, Vinayakumar Gedi, Su-Jeong Park, Myeong-Ae Kim, Min-Kyoung Kim, Hyun-Jung Kwon, Byung-Hoon Cho, Tae-Wan Kim, Kwang-Jick Lee, Chae-Mi Lim
ABSTRACT

The Korean National Residue Programme comprises three different approaches for evaluating domestic and imported foods of animal origin: monitoring, surveillance/enforcement and an exploratory test programme. Monitoring and surveillance/enforcement testing programmes are routinely implemented by 17 Provincial Veterinary Services for domestic products and regional offices of the Animal and Plant Quarantine Agency (QIA) for imported products. The exploratory project conducted at QIA headquarters is designed to test substances that are not included in monitoring and enforcement testing programmes. Here, we carried out exploratory testing for determining the presence of 42 veterinary drugs that have no established Korean maximum residue limits and analysed their levels simultaneously, in a total of 3108 samples of domestic and imported animal-origin foods. Of the tested drugs, acetylsalicylic, paracetamol, clopidol, diclazuril, amprolium, toltrazuril and its metabolites (toltrazuril sulphone and toltrazuril sulphoxide) and phenylbutazone and its metabolites (oxyphenylbutazone) were detected.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Acetonitrile solution, contains 0.05 % (w/v) ammonium formate, 5 % (v/v) water, 0.1 % (v/v) formic acid, suitable for HPLC
Sigma-Aldrich
Acetic acid, 99.5-100.0%
Sigma-Aldrich
Acetic acid, SAJ first grade, ≥99.0%
Sigma-Aldrich
Acetic acid, JIS special grade, ≥99.7%
Sigma-Aldrich
Acetic acid solution, 1 M, 1 N
Sigma-Aldrich
Acetic acid, ≥99.7%
Sigma-Aldrich
Acetic acid, ≥99.7%
Sigma-Aldrich
Acetic acid, for luminescence, BioUltra, ≥99.5% (GC)
Sigma-Aldrich
Acetic acid, ≥99.5%, FCC, FG
Sigma-Aldrich
Acetic acid, natural, ≥99.5%, FG
Sigma-Aldrich
Ethylene, ≥99.5%
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Ethylene, 99.99%
Sigma-Aldrich
Acetic acid-12C2, 99.9 atom % 12C
Sigma-Aldrich
Acetonitrile solution, contains 0.1 % (v/v) trifluoroacetic acid, suitable for HPLC
Sigma-Aldrich
Acetonitrile solution, contains 0.05 % (v/v) trifluoroacetic acid
Sigma-Aldrich
Acetonitrile solution, contains 0.1 % (v/v) formic acid, suitable for HPLC
Sigma-Aldrich
Phenylbutazone
Sigma-Aldrich
Prednisolone, ≥99%
Sigma-Aldrich
Amprolium hydrochloride
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Prednisone, ≥98%
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Acetylsalicylic acid, ≥99.0%
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Acetylsalicylic acid, analytical standard
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Acetonitrile solution, contains 10.0% acetone, 0.05% formic acid, 40.0% 2-propanol
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Acetic acid, ≥99.7%, suitable for amino acid analysis
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Acetonitrile, HPLC Plus, ≥99.9%, poly-coated bottles
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Acetonitrile, for residue analysis, JIS 5000
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Acetonitrile, for chromatography
Sigma-Aldrich
Acetonitrile, SAJ first grade, ≥99.0%
Sigma-Aldrich
Acetonitrile, JIS special grade, ≥99.5%
Sigma-Aldrich
Acetonitrile, ≥99.8%, for residue analysis, JIS 300