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  • Lipase catalyzed synthesis of benzyl acetate in solvent-free medium using vinyl acetate as acyl donor.

Lipase catalyzed synthesis of benzyl acetate in solvent-free medium using vinyl acetate as acyl donor.

Bioorganic & medicinal chemistry letters (2006-05-23)
Abir B Majumder, Bhupender Singh, Debjit Dutta, Sushabhan Sadhukhan, Munishwar N Gupta
ABSTRACT

Use of vinyl acetate as acyl donor in transesterification of benzyl alcohol catalyzed by a commercially available lipase (Lipozyme RM IM) gave 100% conversion in 10 min. The excess acyl donor and the enzyme could be recovered and reused. Unlike the chemical catalytic processes, it produced no undesirable side product.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Benzyl acetate, ≥99%
Sigma-Aldrich
Benzyl acetate, ≥99%, FCC, FG
Supelco
Benzyl acetate, analytical standard
Sigma-Aldrich
Benzyl acetate, natural, ≥99%, FCC, FG