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AlkylFluor: Deoxyfluorination of Alcohols.

Organic letters (2016-12-10)
Nathaniel W Goldberg, Xiao Shen, Jiakun Li, Tobias Ritter
ABSTRACT

A practical, high-yielding method for the deoxyfluorination of alcohols is presented using AlkylFluor, a novel salt analogue of PhenoFluor. AlkylFluor is readily prepared on multigram scale and is stable to long-term storage in air and exposure to water. The practicality and applicability of this method is demonstrated with a variety of primary and secondary alcohol substrates.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
2-Chloro-1,3-bis(2,6-diisopropylphenyl)imidazolium chloride, ≥95%