Expedient synthesis of sulfinamides from sulfonyl chlorides.

Expedient synthesis of sulfinamides from sulfonyl chlorides.

The Journal of organic chemistry (2007-01-16)

Michael Harmata, Pinguan Zheng, Chaofeng Huang, Maria G Gomes, Weijiang Ying, Kanok-On Rayanil, Kanok-On Ranyanil, Gayatri Balan, Nathan L Calkins

PMID17221999

摘要

Sulfinamides were synthesized from sulfonyl chlorides using a procedure involving in situ reduction of sulfonyl chlorides. The reaction is broad in scope and easy to perform.

材料

產品編號

品牌

產品描述

157767

Sigma-Aldrich

磺酰氯, 97%

278505

Sigma-Aldrich

氯化硫酰溶液, 1.0 M in methylene chloride