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24154

Supelco

VOCOL® Capillary GC Column

L × I.D. 60 m × 0.25 mm, df 1.50 μm

Synonym(s):

FS CAP VOCOL® 60M 1.5UM .25MM

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About This Item

UNSPSC Code:
41115710
eCl@ss:
32119290

material

fused silica

Quality Level

100

Agency

EPA TO-17,502.2,624,8015,8260,OLM04.2 VOA,524.2
NIOSH 1003
suitable for EPA 601

parameter

≤25-250 °C temperature (isothermal or programmed)

Beta value

42

df

1.50 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

60 m × 0.25 mm

application(s)

environmental
food and beverages
forensics and toxicology
industrial hygiene

column type

capillary intermediate polar

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General description

Application: This intermediate polarity column, designed for analyses of volatile organic compounds (VOCs), offers great retention and resolution of highly volatile compounds. Use this column in direct injection ports or coupled to purge and trap systems.
USP Code: None
Phase:
  • Bonded
  • Proprietary
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: Subambient to 250 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: Subambient to 230 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: Subambient to 250 °C (isothermal or programmed)
  • ≥0.53 mm I.D., ≥2 μm: Subambient to 230 °C (isothermal or programmed)

Application

VOCOL® column (diphenyl dimethyl polysiloxane with crosslinking moieties) may be used for their relevancy to the purge-and-trap technique and GC/MS analysis of 34 volatile organics. It was also found suitable in being used for determination of volatile compounds by whole column cryotrapping.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

VOCOL is a registered trademark of Merck KGaA, Darmstadt, Germany

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Certificates of Analysis (COA)

Lot/Batch Number
288185-08
288185-07
288185-06
288185-05
288185-04

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Determination of volatile compounds in water by purging directly to a capillary column with whole column cryotrapping.
Pankow JF and Rosen ME.
Environmental Science & Technology, 22 (4), 398-405 (1988)
Re: Bonilha HS, O'Shields M, Gerlach TT, Deliyski DD. Arytenoid adduction asymmetries in persons with and without voice disorders. Logoped Phoniatr Vocol. 2009 Aug 26:1-7. [E-pub ahead of print].
Gerhard Friedrich
Logopedics, phoniatrics, vocology, 35(3), 149-149 (2009-11-04)
Gulsen Pasa et al.
Logopedics, phoniatrics, vocology, 32(3), 128-140 (2007-09-14)
Voice disorders in teachers have a significant impact on their occupational functioning and well being. Teachers are believed to have a high prevalence of voice problems because of the unfavourable acoustic environments in which they work and the high vocal
Ben Barsties et al.
Logopedics, phoniatrics, vocology, 41(1), 27-32 (2014-08-05)
The aim of the study was to determine the impact of body height on speaking fundamental frequency (SF0) while controlling for as many as possible influencing factors such as habits, biophysical conditions, medication, diseases, and others. Fifty-eight females were analyzed
Svante Granqvist et al.
Logopedics, phoniatrics, vocology, 40(3), 113-121 (2014-05-29)
Phonation into glass tubes ('resonance tubes'), keeping the free end of the tube in water, has been a frequently used voice therapy method in Finland and more recently also in other countries. The purpose of this exploratory study was to
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Protocols

Improved Determination of Volatile Organic Compounds in Water by SPME and GC/MS: ISO Standard 17943

High performance, reliability, and reproducibility of HS-SPME in combination with GC/MS for the determination of VOCs in water was proven in an interlaboratory trial. The new ISO 17943 using HS-SPME is an improvement on existing official methods for this determination in terms of sensitivity and selectivity.

Improved Determination of Volatile Organic Compounds in Water by SPME and GC/MS: ISO Standard 17943

High performance, reliability, and reproducibility of HS-SPME in combination with GC/MS for the determination of VOCs in water was proven in an interlaboratory trial. The new ISO 17943 using HS-SPME is an improvement on existing official methods for this determination in terms of sensitivity and selectivity.

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Chromatograms

suitable for GC, application for air monitoring

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