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G003642

GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber

suitable for GC, application for SPME

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About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: white wine spiked with 50 ppb pesticides
SPME fiber: 85 μm polyacrylate (57304)
extraction: immersion, room temp (30 min)
desorption process: 250 °C for 5 min
column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 60 °C (1 min), 15 °C/min to 100 °C, 7 °C/min to 300 °C (1 min)
MSD interface: 325 °C
scan range: SIM
carrier gas: helium, 0.7 mL/min, constant
liner: 0.75 mm I.D. SPME liner

suitability

application for SPME

application(s)

food and beverages

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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SPME fiber

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analytical column

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