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96-0327

GC Analysis of Solvents in Water on SPB®-1 SULFUR after SPME using 75 μm Carboxen/PDMS Fiber

suitable for GC, application for SPME

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About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: solvents at 20 ppb in 4 mL water + 25% NaCl in 4 mL vial
SPME fiber: carboxen/PDMS, 75 μm (57318)
extraction: immersion, 10 min, rapid stirring
desorption process: 270 °C, 5 min
column: SPB-1 SULFUR, 30 m × 0.32 mm I.D., 4.0 μm film (24158)
oven: 50°C (2 min) to 150°C at 10°C/min
inj. temp.: splitless (closed 2 min), 260°C, 0.75 mm I.D. liner
detector: FID
carrier gas: helium, 30 cm/sec

suitability

application for SPME

application(s)

chemicals and industrial polymers
environmental
forensics and toxicology

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Ethyl acetate
    3-Methyl-2-butanone
    Methanol

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