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Supelco

SPB®-5 Capillary GC Column

L × I.D. 25 m × 0.32 mm, df 0.52 μm

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About This Item

UNSPSC Code:
41115710
eCl@ss:
32119290

material

fused silica

Agency

meets requirements for USP G27 and G36

parameter

-60-320 °C temperature (isothermal or programmed)

Beta value

154

df

0.52 μm

technique(s)

gas chromatography (GC): suitable

L × I.D.

25 m × 0.32 mm

matrix active group

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

column type

capillary non-polar

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General description

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded
  • Poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
  • ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)

Application

It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
J Corwin et al.
Cancer, 43(3), 1007-1013 (1979-03-01)
Solitary plasmacytoma of bone (SPB) and extramedullary plasmacytoma (EMPC) are unusual solitary tumors of plasma cell origin. The clinical differences between these tumors and multiple myeloma are the subject of continued study. This review examines the radiotherapy experience at M.
Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO

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