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54279-U

Supelco

BPE-DNPH solid phase extraction (SPE) Cartridge

volume 3 mL, bed B 270 mg (DNPH-coated silica), bed A 130 mg (2-BPE coated silica), pkg of 50 ea

Synonym(s):

BPE-DNPH cartridge tube

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About This Item

EC Number:
UNSPSC Code:
12190000
NACRES:
NB.24

product name

BPE-DNPH Cartridge, volume 3 mL, bed B 270 mg (DNPH-coated silica), bed A 130 mg (2-BPE coated silica), pkg of 50 ea

Agency

ASTM® D5197
EPA IP-6A,TO-11A (BPE layer acts as a built-in ozone scrubber; not affected by moisture or high humidity conditions.)
NIOSH 2016 (BPE layer acts as a built-in ozone scrubber; not affected by moisture or high humidity conditions.)

description

Dual-layer air sampling device.

composition

bed A, 130 mg (2-BPE coated silica)
bed B, 270 mg (DNPH-coated silica)

packaging

pkg of 50 ea

technique(s)

active air sampling: suitable

volume

3 mL

application(s)

air monitoring
industrial hygiene

storage temp.

2-8°C
2-8°C

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General description

Our innovative BPE-DNPH cartridge is a dual-bed cartridge device designed for sampling of carbonyls in ambient, indoor and industrial atmospheres. Like traditional DNPH sampling devices, carbonyls (e.g. formaldehyde) are trapped onto our high purity 2,4-dinitrophenylhydrazine (LpDNPH) coated silica gel adsorbent and are converted to form stable hydrazone derivatives but offers the advantage of a 1,2-bis(2-pyridyl) ethylene (BPE) silica gel bed in front resulting in a built-in ozone scrubber that is not affected by high humidity or rainy conditions.

It is a well-known problem when sampling airborne carbonyls using DNPH-coated silica gel devices that ozone interferes with their analysis. To remove this ozone interference, traditional ozone scrubbing devices containing 1.5 g of Potassium Iodide (KI) are used in front of the DNPH device to trap the ozone, which causes negative ozone interference. In high humidity environments and rainy conditions, potassium iodide cartridges (or other multiple bed devices containing both potassium iodide and DNPH) result in sample loss, due to moisture condensation and collection inside the device.

Benefits:
  • Integrated ozone scrubber
  • No extra connections
  • No leaking cartridges
  • High Purity adsorbents for better accuracy in trace analysis
  • Low Background
  • Individual packaging in zip seal bag to maximize sample integrity
  • Suitable for NIOSH 2016, EPA TO-11A, EPA IP-6A and ASTM D5197
*Optional: Simultaneous measurement of ozone and carbonyls in one device

Application

BPE-DNPH Cartridge is used as a sampling device for the sampling of volatile organic compounds in surgical smoke samples analyzed by ultra-performance liquid chromatography technique.

Legal Information

ASTM is a registered trademark of American Society for Testing and Materials

Pictograms

Exclamation mark

Signal Word

Warning

Hazard Statements

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3

Target Organs

Respiratory system

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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Health risk to medical personnel of surgical smoke produced during laparoscopic surgery
Dobrogowski M, et al.
International Journal of Occupational Medicine and Environmental Health, 28(5), 831-840 (2015)

Articles

Carbonyl compounds react within the DNPH cartridge to form immobilized hydrazones, which can be subjected to automated desorption and HPLC analysis with UV detection.

Carbonyl compounds react within the DNPH cartridge to form immobilized hydrazones, which can be subjected to automated desorption and HPLC analysis with UV detection.

Carbonyl compounds react within the DNPH cartridge to form immobilized hydrazones, which can be subjected to automated desorption and HPLC analysis with UV detection.

Carbonyl compounds react within the DNPH cartridge to form immobilized hydrazones, which can be subjected to automated desorption and HPLC analysis with UV detection.

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

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