GC Analysis of 1-Methoxy-2-Propylamine Enantiomers (N-Chloroacetyl Derivatives) on Astec^® CHIRALDEX^™ B-PH

column

Astec CHIRALDEX B-PH, 30 m x 0.25 mm I.D., 0.12 μm (71023AST)

oven

120 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 24 psi

injection

1 μL, 80:1 split

sample

3 mg/mL in methanol
peaks 1 & 2: 1-methoxy-2-propylamine enantiomers (N-chloroacetyl derivatives)