GC Analysis of Class 2 Residual Solvents on Equity-1 after SPME using 85 μm Polyacrylate Fiber

sample/matrix

2 mL water + sodium chloride at 25% (pH 11) containing each analyte at 5 ppm, in a 4 mL vial

SPME fiber

85 μm Polyacrylate, 24 ga (57304)

extraction

eated headspace, 60 °C for 5 min

desorption flow

250 °C for 3 min

column

Equity-1, 10 m x 0.20 mm I.D., 1.2 μm (28043-U)

oven

40 °C (0.75 min), 20 °C/min to 200 °C (10 min)

inj. temp.

250 °C

detector

FID

carrier gas

helium, 35 cm/sec @ 40 °

injection

5:1 split

liner

0.75 mm I.D. SPME type