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COO原产地证书/COA分析证书

55437-U

Supel^™ QuE

Name: Supel<SUP>™</SUP> QuE
Brand: SUPELCO

PSA Tube, pack of 50 ea, suitable for EN 15662:2008 per BS, centrifuge tube volume 15 mL , Shaker Compatible

别名:

QuEChERS

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About This Item

分類程式碼代碼:

41115712

NACRES:

NB.21

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材料

polypropylene tube

agency

suitable for BS EN 15662:2008

產品線

Supel^™

成份

magnesium sulfate, 900 mg
Supelclean^™ PSA, 150 mg (Cat. No. 52738-U)

包裝

pack of 50 ea

技術

QuEChERS: suitable

離心管體積

15 mL , Shaker Compatible

基質活性組

PSA phase

應用

food and beverages

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一般說明

分散SPE法，通常也是指"QuEChERS” 方法（快速，简便，便宜，有效，耐用和安全），是一种现代样本准备技术，正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法，食品/农产品样本首先在水溶性溶剂（比如乙腈），在高盐（比如氯化钠和硫酸镁）和或者缓冲试剂（比如柠檬酸盐）存在下，进行提取。高盐能够引起液相分离，而缓冲试剂能够稳定酸碱不稳定杀虫剂。在摇晃和离心之后，有机相部分就进一步用SPE清洁。和传统的SPE管方法不同，在分散SPE中，清洁需要混合大量的SPE（比如Supelclean PSA, ENVI-Carb，和或者Discovery DSC-18）和提取物。在样本清洁后，混合物经过离心，得到的上清可以直接分析，或者在分析前需要很少的处理。

Supelco有一系列的管和离心管，含有预置量的盐和SPE吸附剂，能够支持现今最常用的方法。

相容性

Compatible with most QuEChERS shakers.

適合性

Suitable for food/agricultural samples low in fat, chlorophyll, and carotinoide content. Ideal for clean up of 6 mL extract after initial food extraction and phase partitioning.

法律資訊

Supel is a trademark of Sigma-Aldrich Co. LLC

Supelclean is a trademark of Sigma-Aldrich Co. LLC

儲存類別代碼

13 - Non Combustible Solids

水污染物質分類（WGK）

WGK 1

閃點（°F）

Not applicable

閃點（°C）

Not applicable

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Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables.

Steven J Lehotay et al.

Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)

This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to

Streamlined sample cleanup using combined dispersive solid-phase extraction and in-vial filtration for analysis of pesticides and environmental pollutants in shrimp.

Lijun Han et al.

Analytica chimica acta, 827, 40-46 (2014-05-17)

A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)

Multi-class, multi-residue analysis of pesticides, polychlorinated biphenyls, polycyclic aromatic hydrocarbons, polybrominated diphenyl ethers and novel flame retardants in fish using fast, low-pressure gas chromatography-tandem mass spectrometry.

Yelena Sapozhnikova et al.

Analytica chimica acta, 758, 80-92 (2012-12-19)

A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using

Pesticide analysis in coffee leaves using a quick, easy, cheap, effective, rugged and safe approach and liquid chromatography tandem mass spectrometry: Optimization of the clean-up step.

Maria Teresa Salles Trevisan et al.

Journal of chromatography. A, 1512, 98-106 (2017-07-20)

An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction

Determination of carbamates in edible vegetable oils by ultra-high performance liquid chromatography-tandem mass spectrometry using a new clean-up based on zirconia for QuEChERS methodology.

David Moreno-González et al.

Talanta, 128, 299-304 (2014-07-26)

In this study a fast, selective and sensitive multiresidue method based on QuEChERS methodology has been evaluated and validated for the determination of carbamate pesticides, in edible vegetable oils by UHPLC-MS/MS. A new clean-up sorbent, Supel(TM) QuE Z-Sep(+), has been

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Supel^™ QuE