GC Analysis of a 32-Component Anilines Mix on SLB^®-IL59

column

SLB-IL59, 30 m x 0.25 mm I.D., 0.20 μm (28891-U)

oven

75 °C (2 min), 10 °C/min to 250 °C, 15 °C/min to 300 °C (25 min)

inj. temp.

250 °C

detector

MSD, interface 275 °C, m/z = 30-300

carrier gas

helium, 0.7 mL/min constant

injection

1 μL pulsed splitless (25 psi pulse)

liner

4 mm I.D., split/splitless type, single taper design

sample

Each analyte at 50 μg/mL in methylene chloride