- Glycosylation reaction via a mild and efficient one-pot reaction using doped natural phosphate with iodine as catalyst.
Glycosylation reaction via a mild and efficient one-pot reaction using doped natural phosphate with iodine as catalyst.
Nucleosides, nucleotides & nucleic acids (2007-12-07)
H B Lazrek, D Ouzebla, L Baddi, J J Vasseur
PMID18058543
ABSTRACT
Several alpha/beta-D-ribonucleosides were synthesized in good yields under mild conditions by N-glycosylations of acetyl 2,3,5-tri-O-benzoyl-beta-D-ribofuranose with silylated nucleobases in acetonitrile using NP doped with iodine as catalyst.
MATERIALS
Product Number
Brand
Product Description
Sigma-Aldrich
Hexamethyldisilazane, produced by Wacker Chemie AG, Burghausen, Germany, ≥97.0% (GC)