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20281

Supelco

Florisil®

100-200 mesh, fine powder

Synonym(s):

Activated magnesium silicate, Magnesium silicate

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About This Item

Empirical Formula (Hill Notation):
MgO3Si
CAS Number:
1343-88-0
Molecular Weight:
100.39
EC Number:
215-681-1
MDL number:
MFCD00078249
UNSPSC Code:
23201100
PubChem Substance ID:
24852120

grade

standard

form

fine powder

packaging

jar of 454 g

technique(s)

LPLC: suitable

surface area

289 m2/g

matrix

Magnesium silicate hydrate

matrix active group

magnesium silicate hydrate

particle size

100-200 mesh
74-149 μm

pore size

60 Å mean pore size

separation technique

hydrophilic interaction (HILIC)

SMILES string

[Mg++].[O-][Si]([O-])=O

InChI

1S/Mg.O3Si/c;1-4(2)3/q+2;-2

InChI key

FKHIFSZMMVMEQY-UHFFFAOYSA-N

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General description

Florisil, adsorbent for the separation of lipids is a commercially-prepared magnesia silica gel. It has a coarse mesh size which helps in rapid flow rate. Florisil is effective in promoting [1,3]-sigmatropic shift of myceophenolic acid related allyl phenyl ethers. Florisil cartridges are used in atmospheric sampling to assess possible interference from air contaminants.

Application

Florisil was used:
  • as column packing material in column chromatography
  • as an adsorbent in gas chromatography with electron capture detector (GC/ECD), capillary column chromatography, adsorption column chromatography
  • in clean-up procedures in gas chromatography-tandem mass spectrometry and GC-FID

Legal Information

Florisil is a registered trademark of U.S. Silica Company

Storage Class

13 - Non Combustible Solids

wgk_germany

nwg

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Eyeshields, Gloves, type N95 (US)

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Certificates of Analysis (COA)

Lot/Batch Number
188962
179650
177531
176929
173562

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An improved gas chromatographic method for the determination of perfluorocarbon tracers in the atmosphere
Lagomarsino, Raymond J.
Journal of Chromatographic Science, 34, 405-412 (1996)
P A de Paula Pereira et al.
Talanta, 49(2), 245-252 (2008-10-31)
A new sampling protocol was developed to determine methanol and ethanol in the gas phase, at low concentration levels, in urban atmospheres. The procedure involves collection of air samples (20.0-30.0 l) with three florisil cartridges connected in series, at a
Determination of atmospheric perfluorocarbon background concentrations of fL/L range at the western coastal area of Korea
Kim, HyeKyeong, et al.
Atmospheric Environment, 1, 4-4 (2002)
R C Prados-Rosales et al.
Journal of chromatography. A, 993(1-2), 121-129 (2003-05-09)
A rapid analytical method for determination of organochlorine pesticide residues in sunflower seeds based on focused microwave-assisted Soxhlet extraction has been developed. The main factors affecting the extraction efficiency--namely microwave power, irradiation time, volume of extractant and number of cycles--were
The covalently bound flavin of Chromatium cytochrome c552. 1. Evidence for cysteine thiohemiacetal at the 8 alpha position.
W H Walker et al.
European journal of biochemistry, 48(2), 439-448 (1974-10-02)
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