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G005266

US EPA Method TO-13: GC Analysis of PAHs on SLB®-5ms

suitable for GC

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 60 °C (1 min), 10 °C/min to 340 °C (5 min)
inj. temp.: 250 °C
MSD interface: 330 °C 300 °C / 200 °C (source/quads)
scan range: m/z 40-450
carrier gas: helium, 1.5 mL/min. constant
injection: 1.5 μL, pulsed (25 psi until 0.2 min) splitless (0.75 min)
liner: 2 mm I.D. FocusLiner™ liner (2879601-U)
sample: 22 component TO-13 standard plus 5 internal standards at 500 ppb in hexane:ethyl ether (90:10)

application(s)

environmental
industrial hygiene

Legal Information

FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Naphthalene
    Acenaphthylene
    Acenaphthene
    Fluorene
    Phenanthrene
    Anthracene
    Fluoranthene
    Pyrene
    Chrysene
    Benzo[b]fluoranthene
    Benzo[k]fluoranthene
    Benzo[a]pyrene
    Benzo[e]pyrene
    Perylene
    Benzo[ghi]perylene
    Coronene
    See All (16)

accessory

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Description
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analytical column

Product No.
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guard column

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Description
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standard

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335355

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47548-U

EPA 8270 GC-MS Tuning Solution II, certified reference material, 1000 μg/mL each component in dichloromethane

48079

Perylene solution, certified reference material, 2000 μg/mL in dichloromethane

21235-U

ORBO™ 2500 Precleaned Large PUF/Amberlite™ XAD®-2/PUF Cartridge, O.D. × L 6.5 cm × 125 mm, pkg of 1 ea

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EPA 8270 Semivolatile Internal Standard Mix, certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mL

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Polynuclear Aromatic Hydrocarbons Mix, certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride: benzene (1:1)

CRM48743

EPA 610 Polynuclear Aromatic Hydrocarbons Mix, certified reference material, in methanol: methylene chloride (1:1) (varied concentration)

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