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28471-U

Supelco

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Synonym(s):

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54

material

fused silica

Agency

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

reg. compliance

FDA LIB 4423

parameter

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Beta value

250

df

0.25 μm

technique(s)

GC/MS: suitable
gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary non-polar

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General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Chemical Characterization of Three Accessions of Brassica juncea L. Extracts from Different Plant Tissues
Oulad El Majdoub Y, et al.
Molecules (Basel), 25(22), 5421-5421 (2020)
Lorenzo Cucinotta et al.
Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction
Annie Xu Zeng et al.
Analytica chimica acta, 803, 166-173 (2013-11-13)
Due to their distinct chemical properties, the application of ionic liquid (IL) compounds as gas chromatography (GC) stationary phases offer unique GC separation especially in the analysis of geometric and positional fatty acid methyl ester (FAME) isomers. Elution behaviour of

Articles

GC Analysis of Neroli Essential Oil on SLB®-5ms

Resolving by Mass

Learn more about how the thermal desorption technique is applied for terpene identification, profiling, odor measurement, industrial hygiene, and environmental emissions.

Sigma-Aldrich presents an article about the analysis of melamine and related compounds in dog food with the use of more economical gas chromatography-mass spectrometry (GC-MS) instrumentation.

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Protocols

GC Analysis of PBDE Flame-Retardant Compounds

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Example displays how MSTFA/MSTFA-d9 derivatization of amphetamine provides valuable information in mass spectra and chromatograms using SLB-5ms GC column.

There are three types of analyses: GRO, DRO, and TPH. The published methods are simply variations of these to meet the different analytical needs of the individual agencies.

Chromatograms

suitable for GCsuitable for GC, application for SPMEsuitable for GC, application for SPMEsuitable for GCShow More

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

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