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G005668

LC/MS Analysis of Antipsychotic Drugs on Ascentis® Express RP Amide

application for HPLC

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About This Item

technique(s)

HPLC: suitable

test parameters

column: Ascentis Express RP Amide, 10 cm x 2.1 mm I.D., 2.7 μm particles (53913-U)
mobile phase: [A] 5 mM ammonium formate water; [B] 5mM ammonium formate in 95:5 (v/v) methanol:water
gradient: held at 35% B for 0.5 min; 35 to 85% B in 5.5 min; held at 85% B for 1 min
flow rate: 0.3 mL/min
pressure: 4641 psi (320 bar)
column temp.: 35 °C
detector: ESI(+), m/z 100-1000
injection: 1 μL
sample: 200 ng/mL in waler

suitability

application for HPLC

application(s)

clinical
pharmaceutical (small molecule)

Legal Information

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    (2S,3S)-Hydroxybupropion hydrochloride, ≥98% (HPLC)
    Bupropion hydrochloride, United States Pharmacopeia (USP) Reference Standard
    Fluphenazine dihydrochloride

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