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Merck

21013-U

Supelco

GC Stationary Phase

phase Bentone 34, bottle of 50 g

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About This Item

Número CE:
Código UNSPSC:
23151817
NACRES:
SB.54

Formulario

solid

envase

bottle of 50 g

Parámetros

0-180 °C temp. range

técnicas

gas chromatography (GC): suitable

grupo activo de la matriz

Bentone 34 phase

solubilidad

toluene: soluble

tipo de columna

packed GC

Descripción general

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients.[1] The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are few parameters that should be considered before choosing a stationary phase.[2] Bentone 34 is a bentonite treated with dimethyloctadecylammonium salts which has broad applications in GC. It can differentiate between isomers of many aromatic compounds and cycloalkane derivatives. It can also be modified with silicone oil in order to improve the peak symmetry.[3]
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.

Aplicación

Bentone 34 may be used as column coating, using a benzene-methanol (9:1) mixture as dispersion agent to analyse cresol mixtures.[4]

Solo componentes del kit

Referencia del producto
Descripción

  • Bentone® 34

Código de clase de almacenamiento

13 - Non Combustible Solids

Clase de riesgo para el agua (WGK)

WGK 2

Punto de inflamabilidad (°F)

Not applicable

Punto de inflamabilidad (°C)

Not applicable

Equipo de protección personal

Eyeshields, Gloves, type N95 (US)


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Visite la Librería de documentos

H. Rotzsche
Stationary Phases in Gas Chromatography (1991)
Analysis of isomeric cresols by gas chromatography.
Nardillo, A. M.,
Chromatographia, 32, 457-460 (1991)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)

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