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Merck

KITALYSIS-24PD

Sigma-Aldrich

KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2

Sinónimos:

Pd Precatalysts

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About This Item

UNSPSC Code:
12161600
NACRES:
NA.22

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings

functional group

phosphine

Application

Screening kit for cross-coupling reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

Downloadable experimental Excel Sheet

Each kit contains 2 customizable screening sets that include the following components:

  • 24 pre-weighed catalysts in glass micro vials loaded with stir bars and topped with cap mat.
  • 2 KitAlysis 24-Well reaction block replacement films.
  • 4 empty substrate stock solution reaction vials with stir bars.
  • 3 stir bars for stock solutions.
  • 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
  • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

signalword

Warning

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - Skin Sens. 1 - STOT SE 3

target_organs

Central nervous system, Respiratory system

supp_hazards

Storage Class

10 - Combustible liquids

flash_point_f

Not applicable

flash_point_c

Not applicable


Certificados de análisis (COA)

Busque Certificados de análisis (COA) introduciendo el número de lote del producto. Los números de lote se encuentran en la etiqueta del producto después de las palabras «Lot» o «Batch»

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Artículos

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

Protocolos

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

Contenido relacionado

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

El diseño y la optimización de reacciones químicas en la síntesis orgánica tiene como objetivo alterar con precisión parámetros de la reacción para conseguir resultados óptimos en la búsqueda de vías hacia moléculas específicas.

Nuestro equipo de científicos tiene experiencia en todas las áreas de investigación: Ciencias de la vida, Ciencia de los materiales, Síntesis química, Cromatografía, Analítica y muchas otras.

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