技術
HPLC: suitable
測試參數
column: Ascentis Express C18, 10 cm x 2.1 mm I.D., 2.7 μm particles (53823-U)
mobile phase: [A] 5 mM ammonium formate, pH 2.5 (titrated with formic acid); [B] methanol
gradient: 5 to 100% B in 10 min
flow rate: 0.4 mL/min
pressure: 4714 psi (325 bar)
column temp.: 35 °C
detector: APCI (+)
injection: 5 μL
sample: 0.15 - 30 mg/L in 90:10, water:acetonitrile
適合性
application for HPLC
應用
food and beverages
分析報告
This application demonstrates the suitability of Ascentis Express C18 for the efficient separation of various toxins.
法律資訊
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Deoxynivalenol
Aflatoxin B1
Aflatoxin B2
Aflatoxin G1
Aflatoxin G2
Aflatoxin M1
Fumonisin B1 solution
Ochratoxin A
Fumonisin B2 solution
Zearalenone
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