測試參數
column: Astec Cellulose DMP, 15 cm x 4.6 mm I.D., 5 μm particles (51098AST)
gradient: Gradient of 5-65% methanol in 3 min, hold for 1 min
mobile phase: [A] CO2; [B] methanol;
flow rate: 4 mL/min
pressure: 1450 psi (100 bar)
column temp.: 35 °C
detector: UV, 220 nm
injection: 5 μL
sample: chlorpheniramine, 2 mg/mL
適合性
application for SFC
應用
pharmaceutical (small molecule)
分析報告
SFC data provided by Dr. Christina Kraml, Lotus Separations, LLC, Princeton, NJ.
Instrument: Berger Analytical SFC system equipped with a dual pump (FCM-1200), autosampler (ALS 3100), column oven (TCM-200) and diode-array detector (DAD-4100); from Mettler Toledo.
Instrument: Berger Analytical SFC system equipped with a dual pump (FCM-1200), autosampler (ALS 3100), column oven (TCM-200) and diode-array detector (DAD-4100); from Mettler Toledo.
法律資訊
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
(±)-Chlorpheniramine maleate salt, ≥99% (perchloric acid titration)
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