47304

Programmed Test Mix

certified reference material, in dichloromethane (varied conc.)

• UNSPSC Code: 12000000

Properties

• grade: certified reference material; TraceCERT^®
• Quality Level: 300
• product line: TraceCERT^®
• CofA: current certificate can be downloaded
• packaging: ampule of 2 mL
• concentration: in dichloromethane (varied conc.)
• technique(s): HPLC: suitable; gas chromatography (GC): suitable
• application(s): petroleum
• format: multi-component solution
• storage temp.: 2-8°C

Description

General description

This test mix is based on the comprehensive mix developed by Grob (Grob, et al., J. Chromatogr. 156 (1978) p. 1). It can be used to measure a column′s affinity for many analyte types:

• The normal alkanes (decane and undecane) measure column efficiency.
• The fatty acid methyl esters (methyl decanoate, methyl laurate, and methyl undecanoate) measure column efficiency.
• The alcohol (1-octanol) and diol (2,3-butanediol) measure the presence of hydrogen-bonding sites (exposed silanols).
• The aldehyde (nonanal) measures saturated aldehyde adsorption by means other than hydrogen-bonding.
• The amine (dicyclohexylamine) measures irreversible adsorption.
• The acid/base pair (2,6-dimethylphenol/2,6-dimethylaniline) measure acid/base surface characteristic.
• The acid/base pair (2-ethylhexanoic acid/dicyclohexylamine) measure acid/base surface characteristic.

Application

Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

Other Notes

This Certified Reference Material (CRM) is produced and certified in accordance with ISO 17034 and ISO/IEC 17025. All information regarding the use of this CRM can be found on the certificate of analysis.

Legal Information

TraceCERT is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

2,3-Butanediol 530 μg/mL
Decane 280 μg/mL
Dicyclohexylamine 310 μg/mL
2,6-Dimethylaniline 320 μg/mL
2,6-Dimethylphenol 320 μg/mL
2-Ethylhexanoic acid 380 μg/mL
Methyl decanoate 420 μg/mL
Methyl laurate 410 μg/mL
Methyl undecanoate 420 μg/mL
Nonanal 400 μg/mL
1-Octanol 360 μg/mL
Undecane 290 μg/mL
See All (12)

Safety Information

• Pictograms: GHS08,GHS07
• Signal Word: Warning
• Hazard Statements: H315,H319,H336,H351,H412
• Precautionary Statements: P202 - P261 - P273 - P302 + P352 - P305 + P351 + P338 - P308 + P313
• Hazard Classifications: Aquatic Chronic 3 - Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
• Target Organs: Central nervous system
• Storage Class Code: 6.1D - Non-combustible acute toxic Cat.3 / toxic hazardous materials or hazardous materials causing chronic effects
• WGK: WGK 2
• Flash Point(F): Not applicable
• Flash Point(C): Not applicable