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556645

Sigma-Aldrich

N-Heptafluorobutyrylimidazole

97%

Synonym(s):

1-(Perfluorobutyryl)imidazole, NSC 151966

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About This Item

Empirical Formula (Hill Notation):
C7H3F7N2O
CAS Number:
32477-35-3
Molecular Weight:
264.10
EC Number:
251-063-8
MDL number:
MFCD00014503
UNSPSC Code:
12352005
PubChem Substance ID:
24879570
NACRES:
NA.22

Quality Level

100

Assay

97%

refractive index

n20/D 1.3865 (lit.)

bp

161 °C (lit.)

density

1.490 g/mL at 25 °C (lit.)

storage temp.

2-8°C

SMILES string

FC(F)(F)C(F)(F)C(F)(F)C(=O)n1ccnc1

InChI

1S/C7H3F7N2O/c8-5(9,6(10,11)7(12,13)14)4(17)16-2-1-15-3-16/h1-3H

InChI key

MSYHGYDAVLDKCE-UHFFFAOYSA-N

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General description

May form a precipitate and may darken on storage-will not effect performance.

Application

N-Heptafluorobutyrylimidazole may be used as a derivatization reagent in the gas-liquid chromatographic (GLC) analysis of the following compounds:
  • deoxynivalenol in wheat
  • antibiotics (gentamicin, tobramycin, netilmicin, and amikacin) in human serum
  • melatonin
  • heptafluorobutyryl compounds formed by acylation of indolealkylamines
  • acylation products of of morphine, codeine and nalorphine

Storage Class Code

10 - Combustible liquids

WGK

WGK 3

Flash Point(F)

170.6 °F - closed cup

Flash Point(C)

77 °C - closed cup

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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P M Scott et al.
Journal - Association of Official Analytical Chemists, 64(6), 1364-1371 (1981-11-01)
A method for determining deoxynivalenol (DON) in wheat has been developed in conjunction with an assessment of contamination in Canada. The sample is extracted with methanol-water; the extract is treated with 30% aqueous ammonium sulfate solution and extracted with 4
A gas-liquid chromatographic assay of melatonin and indoleamines using heptafluorobutyryl derivatives.
P H Degen et al.
Analytical biochemistry, 45(2), 634-644 (1972-02-01)
A Fidder et al.
Archives of toxicology, 74(4-5), 207-214 (2000-08-26)
The development of a procedure for retrospective detection and quantitation of exposure to the arsenical dichloro(2-chlorovinyl)arsine (lewisite; L1) has been initiated. Upon incubation of human blood with [14C]L1 (20 nM-0.2 mM) in vitro, more than 90% of the total radioactivity
Y Luo et al.
Journal of chromatography. B, Biomedical applications, 667(2), 344-348 (1995-05-19)
A method for the monitoring of dihydroetorphine hydrochloride, a powerful anaesthetic and analgesic drug, in biological fluids was developed, involving GC-MS with multiple selected-ion monitoring. Dihydroetorphine was extracted from human blood and urine with dichloromethane and then derivatized with N-heptafluorobutyrylimidazole
Xinxin Li et al.
Colloids and surfaces. B, Biointerfaces, 74(1), 370-374 (2009-09-01)
Patterning of neural stem cells (NSCs) is of great importance for its potential applications in the therapy of nerve injuries. Due to the critical requirements and the great difficulty in NSCs cultivation, developing new methods for NSCs patterning is very
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