GC Analysis of Class 3 Residual Solvents on OVI-G43
CONDITIONS
column
OVI-G43, 30 m x 0.53 mm I.D., 3.0 μm with 5 m intermediate polarity guard (25396)
oven
35 Ā°C (15 min), 5 Ā°C/min to 200 Ā°C
inj. temp.
225 Ā°C
detector
FID, 250 Ā°C
carrier gas
helium, 30 cm/sec @ 35 Ā°C
injection
1 μL 33:1 split
liner
single taper
sample
27 analytes, each at 3000 μg/mL in methanol