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2,2-Dimethoxypropane

analytical standard

Synonym(s):

Acetone dimethyl acetal

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About This Item

Linear Formula:
(CH3)2C(OCH3)2
CAS Number:
Molecular Weight:
104.15
Beilstein:
635678
EC Number:
MDL number:
UNSPSC Code:
41116107
PubChem Substance ID:
NACRES:
NA.02

grade

analytical standard

Quality Level

vapor density

3.59 (vs air)

vapor pressure

60 mmHg ( 15.8 °C)

Assay

≥99.4% (GC)

shelf life

limited shelf life, expiry date on the label

expl. lim.

31 %, 58 °F
6 %, 27 °F

technique(s)

HPLC: suitable
gas chromatography (GC): suitable

refractive index

n20/D 1.378 (lit.)
n20/D 1.378

bp

79-81 °C
83 °C (lit.)

density

0.847 g/mL at 25 °C (lit.)

application(s)

environmental

format

neat

SMILES string

COC(C)(C)OC

InChI

1S/C5H12O2/c1-5(2,6-3)7-4/h1-4H3

InChI key

HEWZVZIVELJPQZ-UHFFFAOYSA-N

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General description

2,2-Dimethoxypropane is an organic compound, which may be used as a protecting agent in the process of the synthesis of structurally related alkaloids like narciclasine and lycoricidine using phenylbromide as the starting material.

Application

2,2-Dimethoxypropane may be used as an analytical standard for the determination of the analyte in biological samples by headspace gas chromatography-mass spectrometry (HS-GC/MS) technique.
Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

Pictograms

FlameExclamation mark

Signal Word

Danger

Hazard Statements

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 2

Supplementary Hazards

Storage Class Code

3 - Flammable liquids

WGK

WGK 2

Flash Point(F)

14.0 °F - closed cup

Flash Point(C)

-10 °C - closed cup

Personal Protective Equipment

dust mask type N95 (US), Eyeshields, Gloves

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Certificates of Analysis (COA)

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Total Synthesis of Lycoricidine and Narciclasine by Chemical Dearomatization of Bromobenzene
Southgate.HE, et al.
Angewandte Chemie (Weinheim an der Bergstrasse, Germany), 129(47), 15245-15248 (2017)
Quantitative determination of n-propane, iso-butane, and n-butane by headspace GC-MS in intoxications by inhalation of lighter fluid
Bouche MPLA, et al.
Journal of Analytical Toxicology, 26(1), 35-42 (2002)
H J Beckmann et al.
Histochemistry, 76(3), 407-412 (1982-01-01)
Dehydration with 2,2-dimethoxypropane acidified with either 1 N HCL or 0.05 N HCL in an 1:100 ratio has been found to extract various biologically active lipids. The effect is enhanced by an increased proton concentration and seems to occur only
[Quantitative double-labeled autoradiography by chemical washing method using 2,2-dimethoxypropane].
H Sumiya et al.
Kaku igaku. The Japanese journal of nuclear medicine, 24(3), 315-318 (1987-03-01)
Akito Takeuchi et al.
Biomedical chromatography : BMC, 24(5), 465-471 (2009-08-19)
A method for routinely determination of dimethyl sulfoxide (DMSO) and dimethyl sulfone (DMSO(2)) in human urine was developed using gas chromatography-mass spectrometry. The urine sample was treated with 2,2-dimethoxypropane (DMP) and hydrochloric acid for efficient removal of water, which causes

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