493880

(3aS,7R,7aS)-7,7a-Dihydro-7-hydroxy-2,2-dimethyl-1,3-benzodioxol-4(3aH)-one

0.2 g/mL in 0.1 M phosphate buffer, 98%

• 실험식(Hill 표기법): C₉H₁₂O₄
• CAS Number: 139013-57-3
• Molecular Weight: 184.19
• MDL number: MFCD01863551
• UNSPSC 코드: 12352103

속성

• 분석: 98%
• 농도: 0.2 g/mL in 0.1 M phosphate buffer
• pH: 8.5(adjusted to)
• SMILES string: CC1(C)O[C@H]2[C@H](O)C=CC(=O)[C@H]2O1

설명

물리적 형태

A suspension in phosphate buffer.

재구성

To recover the pure product from the suspension:
(1)Thaw the frozen suspension and filter the solid. (2) Rinse bottle with a few milliliters of base-washed (aqueous Na₂CO₃) ethyl acetate. (3) Use the rinsing to wash the solid. (4) Collect solid. (5) To further collect more product from the filtrate: extract filtratewith equal volumes of base-washed (aqueous Na₂CO₃) ethyl acetate (repeat three times). (6) Dry the ethyl acetate extract over MgSO₄. (7) Evaporate the solvent - DO NOT HEAT! (8) Combine solids collected from the suspension and the filtrate. Pure crystals should be stored at -78° C. A suspension of the product in phosphate buffer is stable at 0° C.