추천 제품
분석
≥99%
정제법
sublimation
mp
160-162 °C (lit.)
SMILES string
OC(=O)c1ccccc1I
InChI
1S/C7H5IO2/c8-6-4-2-1-3-5(6)7(9)10/h1-4H,(H,9,10)
InChI key
CJNZAXGUTKBIHP-UHFFFAOYSA-N
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일반 설명
2-Iodobenzoic acid is a halogen substituted carboxylic acid.
애플리케이션
2-Iodobenzoic acid may be used for the following studies:
- One-pot synthesis of hypervalent iodine reagent in the presence of trichloroisocyanuric acid (oxidant). This reagent is employed for the electrophilic trifluoromethylation reactions.
- Synthesis of 1-arylbenziodoxolones.
- Synthesis of isocoumarin.
- Preparation of 2-iodoxybenzoic acid, using oxone (2KHSO5-KHSO4-K2SO4).
신호어
Danger
유해 및 위험 성명서
Hazard Classifications
Acute Tox. 4 Oral - Eye Dam. 1 - Skin Irrit. 2 - STOT SE 3
표적 기관
Respiratory system
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
개인 보호 장비
dust mask type N95 (US), Eyeshields, Gloves
Václav Matoušek et al.
The Journal of organic chemistry, 78(13), 6763-6768 (2013-06-06)
Simplified syntheses suited for large scale preparations of the two hypervalent iodine reagents 1 and 2 for electrophilic trifluoromethylation are reported. In both cases, the stoichiometric oxidants sodium metaperiodate and tert-butyl hypochlorite have been replaced by trichloroisocyanuric acid. Reagent 1
Hypervalent iodine reagents for the oxidation of alcohols and their application to complex molecule synthesis.
Tohma H and Kita Y.
Advanced Synthesis & Catalysis, 346(2), 111-124 (2004)
Manab Chakravarty et al.
The Journal of organic chemistry, 71(24), 9128-9138 (2006-11-18)
Coupling reactions of allenylphosphonates (OCH(2)CMe(2)CH(2)O)P(O)CH=C=CRR' [R, R' = H (1a), R = H, R' = Me (1b), R = R' = Me (1c)] with aryl iodides, iodophenol, and iodobenzoic acid in the presence of palladium(II) acetate are investigated and compared
Mekhman S Yusubov et al.
The Journal of organic chemistry, 78(8), 3767-3773 (2013-03-14)
Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one-pot procedure using Oxone (2KHSO5·KHSO4·K2SO4) as an inexpensive and environmentally safe oxidant. This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic
G W Rafter et al.
Biochimica et biophysica acta, 913(2), 195-199 (1987-06-17)
Homogeneous liver pyruvate kinase was reacted with different sulfhydryl reagents, which included o-iodosobenzoate, 5',5'-dithiobis(2-nitrobenzoic acid) and N-ethylmaleimide. Activity determinations of the treated enzyme made with and without Fru(1,6)P2 indicate that the protein contains two sulfhydryl groups per subunit important to
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