テクニック
gas chromatography (GC): suitable
試験パラメータ
column: Equity-1, 60 m x 0.25 mm I.D., 0.25 μm (28047-U)
oven: 50 °C (3 min), 15 °C/min to 265 °C (5 min)
inj. temp.: 250 °C
detector: FID, 265 °C
carrier gas: helium, 30 cm/sec
injection: 0.5 μL, 200:1 split
liner: 4 mm I.D., splitless type, single taper wool packed FocusLiner™ design
sample: reformulated unleaded gasoline
アプリケーション
petroleum
アナリシスノート
This application illustrates the analysis of a sample of reformulated gasoline on the Equity-1 column. Due to the nonpolar nature of the phase, there is a great deal of overlap in the elution ranges of the aliphatic and aromatic portions of this highly complex sample. Benzene is not baseline resolved even on a 60 m column. For this reason, this phase could not be used by itself for the analysis of benzene in this sample.
法的情報
FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
アナライト
詳細
Ethanol denatured
Pentane
Hexane
Benzene
Heptane
Toluene
Octane
Ethylbenzene
p-Xylene
m-Xylene
o-Xylene
Nonane
1,2,4-Trimethylbenzene
Decane
1,2,3-Trimethylbenzene
Undecane
Durene
Naphthalene
2-Methylnaphthalene solution
1-Methylnaphthalene
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