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794-0864

GC Analysis of Residual Solvents on SPB®-624 after SPME using 100 μm PDMS Fiber

suitable for GC, application for SPME

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About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

SPME fiber: polydimethylsiloxane, 100 μm (57300-U)
extraction: headspace or immersion sampling (15 min) 1 min desorption
column: SPB-624, 75 m × 0.53 mm I.D., 3.0 μm (25432)
oven: 40 °C (35 min) to 220 °C at 40 °C/min, hold 5 min
inj. temp.: splitless (closed 3 min), 200 °C
detector: FID, 250 °C
carrier gas: helium, 35 cm/sec

suitability

application for SPME

application(s)

pharmaceutical (small molecule)

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Methanol
    Methylene chloride
    Ethanol
    1,4-Dioxane
    Acetone
    Chloroform
    Trichloroethylene
    Benzene
    See All (8)

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