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55952

Supelco

Fusaric acid

for HPLC derivatization, ≥99.0% (HPLC)

Sinónimos:

5-Butylpicolinic acid, 5-Butylpyridine-2-carboxylic acid

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About This Item

Fórmula empírica (notación de Hill):
C10H13NO2
Número de CAS:
536-69-6
Peso molecular:
179.22
Beilstein/REAXYS Number:
125804
EC Number:
208-643-0
MDL number:
MFCD00006298
UNSPSC Code:
12352204
NACRES:
NA.22

grade

for HPLC derivatization

Quality Level

100

assay

≥99.0% (HPLC)

technique(s)

HPLC: suitable

SMILES string

CCCCc1ccc(nc1)C(O)=O

InChI

1S/C10H13NO2/c1-2-3-4-8-5-6-9(10(12)13)11-7-8/h5-7H,2-4H2,1H3,(H,12,13)

InChI key

DGMPVYSXXIOGJY-UHFFFAOYSA-N

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General description

Fusaric acid is a novel proton-affinitive derivatizing agent, having an ionization moiety and a hydrophobic moiety. It is commonly used for the derivatization of alcohols and phenols, by liquid chromatography coupled with electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS).

Application

Fusaric acid may be used as a derivatizing reagent for the quantification of hydroxysteroids and dehydroepiandrosterone (DHEA) and sulfated DHEA in biological samples using liquid chromatography electrospray-ionization-tandem mass spectrometry (LC/ESI-MS/MS) technique.

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pictograms

Exclamation mark
GHS07

signalword

Warning

hcodes

H302

Hazard Classifications

Acute Tox. 4 Oral

Storage Class

11 - Combustible Solids

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

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Certificados de análisis (COA)

Lot/Batch Number
BCCK7071
BCBT2161

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Chemical derivatization to enhance ionization of anabolic steroids in LC-MS for doping-control analysis
I. Athanasiadou et all.
TrAC, Trends in Analytical Chemistry, 42, 137-156 (2013)
Kouwa Yamashita et al.
Journal of the American Society for Mass Spectrometry, 21(2), 249-253 (2009-11-17)
A highly sensitive derivatization method for liquid chromatography (LC)-electrospray ionization (ESI) tandem mass spectrometry of dehydroepiandrosterone (DHEA), testosterone (T), pregnenolone (P5), and 17alpha-OH-pregnenolone (17-OHP5) was developed based on the use of fusaric acid as a reagent. DHEA, P5, and 17-OHP5
T Santa
Drug discoveries & therapeutics, 7(1), 9-17 (2013-03-26)
Liquid chromatography coupled with electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS) has been frequently utilized for the sensitive and selective determination of the trace level compounds in biological samples. In LC/ESI-MS/MS, chemical derivatization is sometimes used to enhance the detection sensitivity
Sevcan Mamur et al.
Drug and chemical toxicology, 43(2), 149-157 (2018-09-12)
Fusaric acid (FA) is produced by several Fusarium species and is commonly found in grains. This investigation was performed to evaluate the cytotoxic and genotoxic effects of FA either in human cervix carcinoma (HeLa) cell line using 3-(4,5-dimethylthiazolyl-2)-2,5 diphenyltetrazolium bromide
Yasuhiro Shibata et al.
The Journal of steroid biochemistry and molecular biology, 145, 193-199 (2014-05-06)
A reliable and sensitive method for analyzing steroids using liquid chromatography tandem mass spectrometry (LC-MS/MS) is required for research concerning dehydroepiandrosterone (DHEA), which plays a central role in steroid hormone biosynthesis and metabolism. Furthermore, after the first proposal of the

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