Profiling flavor compounds of potato crisps during storage using solid-phase microextraction.

Profiling flavor compounds of potato crisps during storage using solid-phase microextraction.

Journal of chromatography. A (2005-03-03)

A Sanches-Silva, J Lopez-Hernández, P Paseiro-Losada

摘要

Headspace solid-phase microextraction (HS-SPME) was studied as a solvent free alternative method for the extraction and characterisation of volatile compounds in stored potato crisps by capillary gas chromatography coupled with mass detection. Better results were obtained when extraction was carried out at 70 degrees C using a divinylbenzene (DVB)-carboxen (CAR)-polydimethylsiloxane fiber. The fiber was exposed for 20 min (extraction time) to the sample headspace, immediately after an equilibrium time of 5 min (time needed to reach the equilibrium between sample and above headspace). A total of 31 compounds were identified in oxidised potato crisps and resulted mainly from the degradation/rearrangement of lipids and carbohydrates.

材料

货号

品牌

产品描述

57348-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex

57328-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder

57298-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler

57299-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm

57329-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler

20358

Supelco

ORBO^™ Carboxen-564 管, W,F,F separators, O.D. × L 6 mm × 75 mm, pkg of 25 ea, for analyte group MEK (methylethyl ketone)

20355

Supelco

ORBO-78 400/200mg，每包 25 支, W,W,W separators, O.D. × L 6 mm × 110 mm, pkg of 25 ea

25467

Supelco

Carboxen^®1010 多孔层壁涂开管柱, L × I.D. 30 m × 0.53 mm, average thickness 30 μm

57318

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga

10478-U

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 1000, 60-80 mesh, bottle of 10 g

25461

Supelco

Carboxen^® 1006 多孔层壁涂开管柱, L × I.D. 30 m × 0.53 mm, average thickness 30 μm

57335-U

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler

57295-U

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler

57319

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler

24246

Supelco

Carboxen^®1010 多孔层壁涂开管柱, L × I.D. 30 m × 0.32 mm, average thickness 15 μm

57334-U

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber

57343-U

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler

57344-U

Supelco

SPME固相微萃取萃取头 Carboxen/聚二甲基硅氧烷 (CAR/PDMS), d_f 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder

24241-U

Supelco

Carboxen^® 1006 多孔层壁涂开管柱, L × I.D. 30 m × 0.32 mm, average thickness 15 μm

54041-U

Supelco

Carboxen^® 1000 双向固相萃取管, 200 mg/mL, pk 30

11072-U

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 572, 20-45 mesh, bottle of 10 g

10477-U

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 1000, 40-60 mesh, bottle of 50 g

57914-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), for use with autosampler, needle size 23 ga, metal alloy fiber, fiber L 2 cm

28718-U

Supelco

Tenax^® TA/Carboxen^® 1018, glass TD tube, preconditioned, O.D. × L 1/4 in. × 3 1/2 in., Sealed with (Swagelok^® End-Fittings), pkg of 10 ea

10269

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 569, 20-45 mesh, bottle of 10 g

10471

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 1003, 40-60 mesh, bottle of 10 g

23446-U

Supelco

ORBO^™-93吸附管, ORBO tube I.D. × L 6 mm × 95 mm, Bed A 180 mg, Bed B 90 mg, 60/80 mesh, pkg of 25 ea

57912-U

Supelco

SPME 纤维组件二乙烯基苯/羧基/聚二甲基硅氧烷 (DVB/CAR/PDMS), for use with autosampler, needle size 23 ga, metal alloy fiber, fiber L 1 cm

11048-U

Supelco

Carbopack^®吸附剂, matrix Carboxen^® 569, 20-45 mesh, bottle of 500 g

54294-U

Supelco

Carboxen^® 572 for Tobacco Smoke, Adsorbent Bed Wt: 300 mg, cartridge size 3 mL, pkg of 50 ea