Enantio-reversals
CONDITIONS
column
30 m × 0.25 mm I.D., 0.25 μm (α-DEX 24310, β-DEX 24304, γ-DEX 24307)
oven
130 °C
inj. temp.
250 °C
detector
FID, 300 °C
carrier gas
helium, 35 cm/sec
injection
1 μL 100:1 split
sample
1 mg/mL in methylene chloride
30 m × 0.25 mm I.D., 0.25 μm (α-DEX 24310, β-DEX 24304, γ-DEX 24307)
130 °C
250 °C
FID, 300 °C
helium, 35 cm/sec
1 μL 100:1 split
1 mg/mL in methylene chloride