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Merck
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Documentos

33461

Supelco

N-(1-Naphthyl)ethylenediamine dihydrochloride

for determination of sulfonamide and nitrite, ACS reagent, ≥98%

Sinónimos:

2-(1-Naphthylamino)ethylamine dihydrochloride

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About This Item

Fórmula lineal:
C10H7NHCH2CH2NH2 · 2HCl
Número de CAS:
1465-25-4
Peso molecular:
259.17
Beilstein/REAXYS Number:
3707471
EC Number:
215-981-2
MDL number:
MFCD00012556
UNSPSC Code:
41116105
PubChem Substance ID:
329754555
NACRES:
NA.21

grade

ACS reagent
for determination of sulfonamide and nitrite

Quality Level

200

assay

≥98% (calc with ref. to anhyd. subst.)
≥98%

form

powder

technique(s)

UV/Vis spectroscopy: suitable

impurities

≤5% water (Karl Fischer)

mp

194-198 °C (dec.) (lit.)

suitability

complies for identity

SMILES string

Cl.Cl.NCCNc1cccc2ccccc12

InChI

1S/C12H14N2.2ClH/c13-8-9-14-12-7-3-5-10-4-1-2-6-11(10)12;;/h1-7,14H,8-9,13H2;2*1H

InChI key

MZNYWPRCVDMOJG-UHFFFAOYSA-N

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Application

N-(1-Naphthyl)ethylenediamine dihydrochloride dissolved in sulfuric acid-methanol may be used as a reagent for the determination of sugar on thin layer plates. It may also be used for the determination of sub-micromolar concentrations of nitrite ion after diazotisation with sulphanilic acid at low pH, by differential-pulse polarography. It may also be used as the coupling agent for the spectrophotometric determination of aniline by the diazotization-coupling method.

pictograms

Exclamation mark
GHS07

signalword

Warning

hcodes

H315,H319

Hazard Classifications

Eye Irrit. 2 - Skin Irrit. 2

Storage Class

11 - Combustible Solids

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

dust mask type N95 (US), Eyeshields, Gloves

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Certificados de análisis (COA)

Lot/Batch Number
BCCM4379
BCCL6973
BCCL1166
BCCM3100
BCCJ9837

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Spectrophotometric determination of aniline by the diazotization-coupling method with N-(1-naphthyl) ethylenediamine as the coupling agent.
Norwitz G and Keliher PN.
Analytical Chemistry, 53 (8), 1238-1240 (1981)
Determination of nitrite ion by differential-pulse polarography using N-(1-naphthyl) ethylenediamine.
Sabharwal S.
Analyst, 115 (10), 1305-1307 (1990)
N-(1-Naphthyl) ethylenediamine dihydrochloride as a new reagent for nanomole quantification of sugars on thin-layer plates by a mathematical calibration process.
Bounias M.
Analytical Chemistry, 106 (2), 291-295 (1980)
Shigenori Nakano et al.
Talanta, 81(3), 786-791 (2010-03-20)
A novel flow-injection spectrophotometry has been developed for the determination of molybdenum(VI) at nanograms per milliliter levels. The method is based on the catalytic effect of molybdenum(VI) on the bromate oxidative coupling of p-hydrazinobenzenesulfonic acid with N-(1-naphthyl)ethylenediamine to form an
P K Laikind et al.
Analytical biochemistry, 156(1), 81-90 (1986-07-01)
The Bratton-Marshall reaction can be used to identify patients with adenylosuccinate lyase deficiency. These patients excrete in their urine the dephosphorylated derivative of the de novo purine synthesis intermediate 5'-phosphoribosyl-4-(N-succinylcarboxamide)-5-aminoimidazole (SAICAR). The test described here depends on a coupling reaction
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