24037
SPB®-5 Capillary GC Column
L × I.D. 60 m × 0.25 mm, df 1.00 μm
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About This Item
UNSPSC Code:
41115710
eCl@ss:
32119290
Recommended Products
material
fused silica
Quality Level
Agency
meets requirements for USP G27 and G36
parameter
-60-320 °C temperature (isothermal or programmed)
Beta value
63
df
1.00 μm
technique(s)
gas chromatography (GC): suitable
L × I.D.
60 m × 0.25 mm
matrix active group
Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase
column type
capillary non-polar
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General description
Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
USP Code: This column meets USP G27 and G36 requirements.
Phase:
- Bonded
- Poly(5% diphenyl/95% dimethyl siloxane)
- ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
- ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
- ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
- ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)
Application
SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may also be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. Furthermore, it may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.
Other Notes
We offer a variety of chromatography accessories including analytical syringes
Legal Information
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
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P M Scott et al.
Journal - Association of Official Analytical Chemists, 69(5), 889-893 (1986-09-01)
Nivalenol (NIV) is an important Fusarium mycotoxin shown to occur naturally in grains from several countries. Extraction and cleanup procedures previously described for trichothecene analysis have been modified to give good recoveries of NIV from cereal products. The extraction solvent
H J Chou
Journal of AOAC International, 81(5), 943-947 (1998-10-17)
Diethanolamine (DEA) is a precursor of N-nitrosodiethanolamine (NDELA), an animal carcinogen. A gas chromatographic (GC) method was developed for determining DEA in fatty acid diethanolamides that are commonly used in cosmetic products. Methanolic solutions of the amides were analyzed by
S Hasnain et al.
Environmental pollution (Barking, Essex : 1987), 81(2), 179-184 (1993-01-01)
Five Pseudomonad strains, SPb-1, SPb-2, SPb-3, (from a water sample), SPb-4, and SPb-5 (from rhizosphere), which could tolerate lead acetate up to 1000 microm ml(-1), were isolated from an industrially polluted area around Kasoor, Pakistan. Only SPb-5 harbours a lead-resistant
Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
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