8.52062
Fmoc-Tic-OH
Novabiochem®
Synonyme(s) :
Fmoc-Tic-OH, N-1-Fmoc-L-1,2,3,4,-tetrahydro-isoquinoline-3-carboxylic acid
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A propos de cet article
Formule empirique (notation de Hill) :
C25H21NO4
Numéro CAS:
Poids moléculaire :
399.44
UNSPSC Code:
12352209
NACRES:
NA.22
MDL number:
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product line
Novabiochem®
assay
≥97.0% (acidimetric), ≥98% (TLC), ≥98.0% (HPLC)
form
powder
reaction suitability
reaction type: Fmoc solid-phase peptide synthesis
manufacturer/tradename
Novabiochem®
application(s)
peptide synthesis
functional group
Fmoc
storage temp.
15-25°C
SMILES string
N4([C@@H](Cc5c(cccc5)C4)C(=O)[O-])C(=O)OCC1c2c(cccc2)c3c1cccc3
InChI
1S/C25H21NO4/c27-24(28)23-13-16-7-1-2-8-17(16)14-26(23)25(29)30-15-22-20-11-5-3-9-18(20)19-10-4-6-12-21(19)22/h1-12,22-23H,13-15H2,(H,27,28)/p-1/t23-/m0/s1
InChI key
LIRBCUNCXDZOOU-QHCPKHFHSA-M
General description
Standard building block for introduction of Tic amino-acid residues by Fmoc SPPS
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Literature references
[1] M. Vincent, et al. (1982) Tetrahedron Lett., 16, 1677.
[2] P. L. Julian, et al. (1984) J. Am. Chem. Soc., 79, 180.
[3] W. A. Kazmierski, et al. (1988) Tetrahedron Lett., 44, 697.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS
Literature references
[1] M. Vincent, et al. (1982) Tetrahedron Lett., 16, 1677.
[2] P. L. Julian, et al. (1984) J. Am. Chem. Soc., 79, 180.
[3] W. A. Kazmierski, et al. (1988) Tetrahedron Lett., 44, 697.
Analysis Note
Color (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.0 % (a/a)
Purity (TLC(011C)): ≥ 98 %
Purity (TLC(CMA2)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Assay (acidimetric): ≥ 97.0 %
Water (K. F.): ≤ 1.00 %
To see the solvent systems used for TLC of Novabiochem® products please click here.
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.0 % (a/a)
Purity (TLC(011C)): ≥ 98 %
Purity (TLC(CMA2)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Assay (acidimetric): ≥ 97.0 %
Water (K. F.): ≤ 1.00 %
To see the solvent systems used for TLC of Novabiochem® products please click here.
Other Notes
Replaces: 04-12-1130
Legal Information
Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany
Classe de stockage
11 - Combustible Solids
Que se passe-t-il ?
WGK 3
Point d'éclair (°F)
Not applicable
Point d'éclair (°C)
Not applicable
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