370452
2,2-Diethoxyacetamide
97%
Synonym(s):
Glyoxylic amide diethyl acetal
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About This Item
Linear Formula:
(CH3CH2O)2CHCONH2
CAS Number:
Molecular Weight:
147.17
Beilstein:
1760414
EC Number:
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
Assay
97%
mp
76-78 °C (lit.)
SMILES string
CCOC(OCC)C(N)=O
InChI
1S/C6H13NO3/c1-3-9-6(5(7)8)10-4-2/h6H,3-4H2,1-2H3,(H2,7,8)
InChI key
DSKGWFQMJHBHRT-UHFFFAOYSA-N
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General description
2,2-Diethoxyacetamide participates in the synthesis of pyridine-containing central domain of the amythiamicin group of thiopeptide antibiotics.
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
Certificates of Analysis (COA)
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Mark C Bagley et al.
Chemical communications (Cambridge, England), (1)(1), 102-103 (2004-01-23)
The pyridine-containing central domain of the amythiamicin group of thiopeptide antibiotics is prepared in protected form in 9 steps, 93%ee and 18% overall yield from (S)-2-[1-(tert-butoxycarbonylamino)-2-methylpropyl]thiazole-4-carboxylic acid by Michael addition-cyclodehydration of a 2-(2-thiazolyl)enamine and 1-(2-thiazolyl)propynone.
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