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97-0183

GC Analysis of Volatiles on VOCOL® after SPME using 75 μm Carboxen/PDMS Fiber

suitable for GC, application for SPME

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About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: 1 ppb each analyte in 3 mL water (25% NaCl added) in 4 mL vial
SPME fiber: Carboxen/PDMS, 75 μm (57318)
extraction: headspace, 40°C (20 min), with stirring
desorption process: 5 min., 310 °C
column: VOCOL®, 30 m × 0.25 mm I.D., 1.5 μm (24205-U)
oven: 40°C (2 min) to 210°C at 8°C/min
detector: ion trap, MS, m/z = 45-260 (0.6sec/scan)
carrier gas: helium, 35 cm/sec
injection: splitless/split (closed 2 min), 0.75 mm I.D. liner

suitability

application for SPME

application(s)

environmental

Legal Information

VOCOL is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    1,4-Dichlorobenzene
    Hexachlorobutadiene
    tert-Butylbenzene
    1,2,3-Trichlorobenzene
    p-Cymene
    Chloromethane
    Tetrachloroethylene
    Trichloroethylene
    sec-Butylbenzene
    1,1-Dichloroethylene
    Fluorobenzene
    4-Chlorotoluene
    Carbon tetrachloride
    Vinyl chloride
    1,3-Dichlorobenzene
    1,1-Dichloropropene
    Bromobenzene
    Bromochloromethane
    cis-1,2-Dichloroethylene
    Bromodichloromethane
    Ethylbenzene
    Styrene
    1,2,4-Trichlorobenzene
    1,2,3-Trichloropropane
    1,1,1,2-Tetrachloroethane
    trans-1,2-Dichloroethylene
    1,3,5-Trimethylbenzene
    m-Xylene
    Dichlorodifluoromethane
    1,2-Dichloroethane
    1,2-Dichlorobenzene
    1,2-Dichlorobenzene-d4
    2,2-Dichloropropane
    Naphthalene
    Chloroform
    1,2-Dibromoethane
    Benzene
    1,1-Dichloroethane
    Propylbenzene
    1,2-Dichloropropane
    2-Chlorotoluene
    Chlorobenzene
    1,1,2,2-Tetrachloroethane
    p-Xylene
    1,2-Dibromo-3-chloropropane
    1,1,1-Trichloroethane
    Toluene
    1,2,4-Trimethylbenzene
    Bromoform
    o-Xylene
    1,1,2-Trichloroethane
    cis-1,3-Dichloropropene
    1,3-Dichloropropane
    Isopropylbenzene, analytical standard, This product has been discontinued but product PHR1210-1.2ml may be an acceptable replacement
    Methylene chloride
    Bromomethane
    trans-1,3-Dichloropropene
    Chloroethane
    Trichlorofluoromethane
    Dibromomethane
    See All (60)

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