LC/MS Analysis of Illicit Bath Salts on Ascentis® Express HILIC, Set 1
Materialien
Analytische Säule
Produkt-Nr.
Beschreibung
Preisangaben
Anwendung
Produkt-Nr.
Beschreibung
Preisangaben
Standard
Produkt-Nr.
Beschreibung
Preisangaben
Methedrone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®3-Methoxymethcathinon -hydrochlorid -Lösung
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®MDPBP hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®Naphyrone hydrochloride
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®Pentylon -hydrochlorid
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U)
mobile phase
5 mM ammonium formate in [A] acetonitrile; [B] water; (98:2, A:B)
flow rate
0.6 mL/min
pressure
267 psi (18.4 bar)
column temp.
35 °C
detector
MS, ESI(+) TOF, Summed Ion Chromatogram
injection
2 μL
sample
500 ng/mL in acetonitrile
Beschreibung
Hinweis zur Analyse
HILIC mode operation on an Ascentis Express column provided baseline resolution of these bath salts, including isobaric compounds. The highest quality LC-MS solvents were used to supply low background interference and low particulate contaminants for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
Rechtliche Hinweise
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany