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Merck

Development of a rapid and accurate method for the determination of key compounds of pig odor.

Journal of chromatography. A (2004-07-06)
Stephanie Willig, Markus Lacorn, Rolf Claus
ZUSAMMENFASSUNG

Sampling of odor substances in the emissions from swine production facilities is still the limiting step for routine odor quantification. Solid sorption techniques based on cartridges were developed for three categories of substances (indoles, volatile fatty acids and methylthiol) and were standardized to a sampling time of 15 min. These cartridges also trap dust particles which transport odor substances. Quantification was performed by RP-HPLC or GC. Reliability criteria revealed excellent values for sensitivity (lower ppb level) and repeatability (R.S.D. < 10%), thus they are comparable to fiber solid-phase micro extraction sorption techniques. Parallel determinations in feces and air revealed high correlations (r = 0.99, P < 0.01), so that microbial processes during digestion determine odor quality and hence provide a possibility to reduce odor via feeding.

MATERIALIEN
Produktnummer
Marke
Produktbeschreibung

Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), needle size 24 ga, StableFlex
Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder
Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm
Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Polydimethylsiloxan (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 23 ga
Supelco
SPME-Faseranordnung Polydimethylsiloxan (PDMS), df 100 μm(PDMS, needle size 24 ga, for use with manual holder
Supelco
SPME-Faseranordnung Polydimethylsiloxan (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 24 ga
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Polyacrylat (PA), df 85 μm(PA, for use with autosampler, needle size 23 ga
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 23 ga, PDMS/DVB StableFlex, for use with autosampler
Supelco
SPME-Faseranordnung Polyacrylat (PA), df 85 μm(PA, for use with autosampler, needle size 24 ga
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with autosampler
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holder
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler
Supelco
SPME-Faseranordnung Polydimethylsiloxan (PDMS), df 100 μm(PDMS, for use with manual holder, needle size 23 ga
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), df 65 μm(PDMS/DVB, for use with autosampler, needle size 23 ga
Supelco
SPME StableFlex Methodenentwicklungs-Kit, for use with manual holder
Supelco
SPME-Faseranordnung Carboxen/Polydimethylsiloxan (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder
Supelco
SPME-Faseranordnung, Carbowax-Polyethylenglycol (PEG)-Beschichtung, needle size 23 ga, df 60 μm(PEG, for use with autosampler
Supelco
SPME StableFlex Methodenentwicklungs-Kit, needle size 23 ga, for use with autosampler
Supelco
SPME-Faseranordnung Polydimethylsiloxan/Divinylbenzen (PDMS/DVB), fused silica fiber, df 65 μm(PDMS/DVB, for use with manual holder, needle size 23 ga
Supelco
SPME-Faseranordnung Polyacrylat (PA), df 85 μm(PA, for use with manual holder, needle size 24 ga
Supelco
SPME-Faseranordnung Divinylbenzol/Carboxen/Polydimethylsiloxan (DVB/CAR/PDMS), for use with autosampler, needle size 23 ga, metal alloy fiber, fiber L 2 cm