No specific information is available regarding the stability of PTAD in acetonitrile solution. Preparation of the solution immediately before use is recommended due to the absence of stability data.
280992
4-Phenyl-1,2,4-triazoline-3,5-dione
97%
Sinónimos:
4-Phenyl-3H-1,2,4-triazole-3,5(4H)-dione, PTAD
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Acerca de este artículo
Fórmula empírica (notación de Hill):
C8H5N3O2
Número CAS:
Peso molecular:
175.14
UNSPSC Code:
12352005
NACRES:
NA.22
PubChem Substance ID:
EC Number:
224-191-7
Beilstein/REAXYS Number:
141548
MDL number:
Assay:
97%
Form:
solid
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Servicio técnico
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Permítanos ayudarleQuality Segment
assay
97%
form
solid
mp
165-170 °C (dec.) (lit.)
storage temp.
2-8°C
SMILES string
O=C1N=NC(=O)N1c2ccccc2
InChI
1S/C8H5N3O2/c12-7-9-10-8(13)11(7)6-4-2-1-3-5-6/h1-5H
InChI key
ISULLEUFOQSBGY-UHFFFAOYSA-N
Application
4-Phenyl-1,2,4-triazoline-3,5-dione (PTAD) can be used as an efficient and selective reagent for the oxidation of thiols to disulfides.
It can also be used:
It can also be used:
- As a dehydrogenating agent to synthesize annulated dihydropyridazines by inverse [4+2] cycloaddition reaction between cyclic alkenes and 1,2,4,5-tetrazines.
- As a dienophile to synthesize cycloaddition products by fast hetero-Diels−Alder reactions.
- As an efficient oxidizing agent for the synthesis of pyridine derivatives from 1,4-dihydropyridines.
- In the synthesis of urazoles via [3+2] cycloaddition with allylsilanes.
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Este artículo | |||
|---|---|---|---|
| assay 97% | assay 99% | assay 97% | assay - |
| Quality Level 100 | Quality Level 200 | Quality Level 100 | Quality Level 200 |
| form solid | form crystals | form solid | form powder |
| mp 165-170 °C (dec.) (lit.) | mp 84-86 °C (lit.) | mp 165-169 °C (lit.) | mp 83-86 °C |
| storage temp. 2-8°C | storage temp. - | storage temp. - | storage temp. 2-30°C |
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Clase de almacenamiento
11 - Combustible Solids
wgk
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
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I use PTAD for derivatisation and dissolve it in ACN. Do you have any information about how long the PTAD remains stable in the ACN solution?
1 answer-
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How can I determine the shelf life / expiration / retest date of this product?
1 answer-
If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdfHelpful?
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How is shipping temperature determined? And how is it related to the product storage temperature?
1 answer-
Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf
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