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G005936

GC Analysis of Volatiles in PVC Pipe on SPB®-HAP after Collection/Desorption using Carbotrap® 300 Tube

suitable for GC, application for air monitoring

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

sample/matrix: (1g PVC pipe Schedule 40)
thermal desorption tube: Carbotrap® 300 Glass-Fritted Thermal Desorption Tube, 1/4 in O.D. x 3.5 in L (30141-U)
dry purge: 60 min
desorption process: 350 °C with 10 min hold
transfer line/valve temp.: 180 °C
column: SPB®-HAP, 60 m x 0.32 mm I.D., 4 μm (25020-U)
oven: 40 °C (3 min), 12 °C/min to 200 °C (20 min)
detector: MSD
MSD interface: 210 °C
carrier gas: helium

suitability

application for air monitoring

application(s)

air monitoring
environmental
industrial hygiene

Analysis Note

Qualitative volatile headspace outgassing of PVC pipe using the ATIS with analysis by thermal desorption.

Legal Information

Carbotrap is a registered trademark of Merck KGaA, Darmstadt, Germany
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description

    Acetone
    Acetic acid
    Ethylene sulfide
    Hexanal
    4-Hydroxy-4-methyl-2-pentanone
    Cumene
    2-Ethyl-1-hexanol
    Decanal
    Nonanoic acid
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