Anilines

column

Equity-5, 30 m × 0.25 mm I.D., 0.25 μm (28089-U)

oven

50 °C (2 min), 10 ºC/min to 200 °C, 15 ºC/min to 325 °C

inj. temp.

250 °C

detector

FID, 325 °C

carrier gas

helium, constant flow, 1.3 mL/sec

injection

1 μL, splitless (0.5 min)

liner

4 mm I.D., single taper

sample

50 ng on-column of a custom anilines mix