55233-U
Supel™ QuE
PSA/ENVI-Carb Tube 2, pk of 50, suitable for EN 15662:2008 per BS
Synonym(s):
QuEChERS
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About This Item
UNSPSC Code:
41115712
NACRES:
NB.21
Recommended Products
Agency
suitable for BS EN 15662:2008
composition
magnesium sulfate, 900 mg
Supelclean™
ENVI-Carb, 45 mg (Cat. No. 57210-U)
Supelclean™
PSA, 150 mg (Cat. No. 52738-U)
packaging
pk of 50
technique(s)
QuEChERS: suitable
centrifuge tube volume
12 mL , Greiner Cat. No. 163270
application(s)
food and beverages
separation technique
normal phase
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General description
Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
Application
Supel™ QuE may be used as a quick, easy, cheap, effective, rugged, safe extraction tube for the dispersive solid phase extraction of pesticide residues in vegetables using acetylcholinesterase (AChE) inhibition assay.
Suitability
Suitable for food/agricultural samples with higher levels of chlorophyll and carotinoides (e.g., red sweet pepper, spinach, lamb′s lettuce, ruccolla, etc.). Ideal for clean up of 6 mL extract after initial food extraction and phase partitioning.
Legal Information
Supel is a trademark of Sigma-Aldrich Co. LLC
Supelclean is a trademark of Sigma-Aldrich Co. LLC
Storage Class Code
11 - Combustible Solids
WGK
WGK 1
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
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Analysis of non-cleaned QuEChERS extracts for the determination of pesticide residues in fruit, vegetables and cereals by gas chromatography-tandem mass spectrometry
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Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment, 33(2), 300-312 (2016)
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Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 46(6), 277-281 (2006-01-31)
An analytical method was developed for the determination of phenmedipham (PM) in agricultural products using reversed-phase high-performance liquid chromatography with UV detection. A sample was extracted with acetonitrile, and the acetonitrile layer was separated by salting-out. The acetonitrile phase was
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Se pu = Chinese journal of chromatography, 30(9), 896-902 (2013-01-05)
A high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/ MS) method was established for the determination of fungicide anilinopyrimidine residues including pyrimethanil, mepanipyrim, and cyprodinil in foodstuffs with series solid phase extraction (SPE). The food sample was first extracted with ethyl
U Führer et al.
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Halogenated anisoles (methyl-phenyl ethers) appear to be ubiquitous organic trace compounds in the environment. An analytical method is presented for analyzing the altogether 134 congeners of chloro-, bromo- and mixed bromochloro-anisoles on an isomer-specific basis in air. High volume sampling
Sachiyo Ibuki et al.
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 48(5), 139-143 (2007-11-22)
A method for simultaneous determination of Dichlorvos (DDVP), Trichlorfon (DEP) and Naled (BRP) in fruits and vegetables by liquid chromatography with tandem mass spectrometry (LC/MS/MS) was developed. Pesticides were extracted with ethyl acetate together with phosphoric acid and anhydrous sodium
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