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12087-U

Supelco

Metal Packed GC Column (General Configuration)

phase 5% Carbowax 20M, matrix 60/80 Carbopack B support, L × O.D. × I.D. 3.0 ft (0.91 m) × 1/16 in. × 1.25 mm, Preconditioned

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About This Item

UNSPSC Code:
41115710
NACRES:
SB.54

material

stainless steel column

parameter

0-225 °C temperature (isothermal or programmed)

technique(s)

gas chromatography (GC): suitable

L × O.D. × I.D.

3.0 ft (0.91 m) × 1/16 in. × 1.25 mm, Preconditioned

matrix

60/80 Carbopack B support

matrix active group

5% Carbowax 20M phase

column type

packed GC

compatibility

for use with General Configuration

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General description

Packed column made up of stainless steel are basically employed when higher carrier gas flow rates are employed as they can sustain elevated pressure. Stainless steel columns are usually washed with dilute hydrochloric acid, then with water followed by methanol, acetone, methylene dichloride and n-hexane in order to remove any corrosion products and traces of lubricating agents. The GC column made up of Carbowax -20M liquid phase on a Carbopack B support packing material is highly efficient, has low bleed and almost no active site. Furthermore, it guarantees uniform packing in the column thereby leading to rapid analysis.
An economical metal column should be used for less demanding applications where the inertness of glass is not required. This column is of a general configuration, and can be carefully bent to fit most instruments.

Application

Carbopack B or graphitized thermal carbon block (GTCB) maybe used for the determination of trace amounts of simazine and atrazine in water. It was also used for the Gas chromatographic evaluation of the organic components present in the atmosphere at trace levels for pre-concentration of the sample.

Other Notes

This is a micropacked column. It is packed full and contains stainless steel screens.

This column is preconditioned.

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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Basic Gas Chromatography-Mass Spectrometry: Principles and Techniques.
Karasek FW and Clement RE.
Science, 15-16 (1988)
Introduction to Analytical Gas Chromatography.
Raymond PW.
Science, 102-108 (1997)
Gas chromatographic evaluation of the organic components present in the atmosphere at trace levels with the aid of carbopack b for pre-concentration of the sample.
Ciccioli, et al.
Journal of Chromatography A, 351, 433-449 (1986)
Rapid determination of simazine and atrazine in water at the parts per trillion (10 (12) level. Extraction by a miniaturized carbopack B trap followed by high-performance liquid chromatography.
Corcia D, et al.
Journal of Chromatography A, 405, 357-363 (1987)

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